i will say Atherton vs donald was one of the great contests in a match.
However for me, Sachin Tendulkar vs Shane Warne, was a mouth watering propect all the time. Two legends of the game going at it. You would have to say though Sachin Came out on top more often than not.
Both are geniuses of the game, but Sachin most of the time out foxed him. When Australia Toured india in 1998, thats probaly the best of the Sachin vs Warne era. The way Sachin Slog swept Warne out of the rough and danced down the track to Warne was exciting. The Classic example being at chennai, where Warne got Sachin out caught behind for only 4, then in the 2 innings, sachin smashed 155, including 5 sixes.
Sachin vs Glen mgrath and Murali have also been exciting to watch. And Sachin vs The Pakistani Quick bowlers.
Other Great contest have been Brian Lara vs glen mgrath and the pakistani quicks. And ricky ponting vs bhaji.
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